A cryogen-consumption-free system for dynamic nuclear polarization at 9.4 T
Abstract
A novel system for dissolution dynamic nuclear polarization based on a cost-effective "cryogen-free" magnet that can generate fields up to 9.4 T with a sample space that can reach temperatures below 1.4 K in a continuous and stable manner. Polarization levels up to P(1H) = 60 ± 5% can be reached with TEMPOL in about 20 min, and P(13C) = 50 ± 5% can be achieved using adiabatic cross polarization.
- Publication:
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Journal of Magnetic Resonance
- Pub Date:
- September 2018
- DOI:
- Bibcode:
- 2018JMagR.294..115B
- Keywords:
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- Dynamic nuclear polarization (DNP);
- Dissolution DNP;
- Cryogen-consumption-free magnets;
- Adiabatic cross polarization