Synthesis and crystal structure of 4-amino-3,5-dinitropyrazole sodium salt
Abstract
A novel energetic material, 4-amino-3,5-dinitropyrazole sodium salt (ADNPNa), was firstly synthesized in a yield of 86.26%. The structure of ADNPNa was confirmed by IR and elemental analysis. The single crystal of ADNPNa was determined by single crystal X-ray diffraction. The crystal belongs to triclinic system, space group P-1 with crystal parameters a=6.284(4)Å, b=6.480(4)Å, c=9.729(6)Å, β= 95.294(9)°, V=365.0(4)Å3, Z=2, μ=0.227mm-1, F(000)= 216, and Dc=1.939g/cm3.
- Publication:
-
Advances in Materials, Machinery, Electronics II
- Pub Date:
- April 2018
- DOI:
- 10.1063/1.5033575
- Bibcode:
- 2018AIPC.1955b0003W