Furnace for Inelastic X‑Ray Scattering from Liquids up to 1600 °C
Abstract
The design and implementation of a furnace for inelastic X‑ray scattering from liquids with sample temperatures up to ≈1600 °C is described. Carbon composite heaters operating in vacuum provide robust heating elements: one pair of heaters has been used for >18 days of operational time above 1500 °C, including eight cycles to room temperature. High‑quality data are obtained to scattering angles as low as 7 mrad in 2θ (Q < 1 nm−1 at 25.7 keV) from a sample at 1560 °C.
- Publication:
-
Physica Status Solidi B Basic Research
- Pub Date:
- November 2020
- DOI:
- 10.1002/pssb.202000093
- arXiv:
- arXiv:2004.14611
- Bibcode:
- 2020PSSBR.25700093B
- Keywords:
-
- Physics - Instrumentation and Detectors;
- Condensed Matter - Materials Science
- E-Print:
- 15 pages, 8 Figures, Proceeding of NCM 14